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CEN/TS 16171:2012

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

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Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)

Withdrawn date

11-03-2023

Superseded by

EN 16171:2016

Published date

21-11-2012

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Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Procedure
8 Calculation
9 Expression of results
10 Performance characteristics
11 Test report
Annex A (informative) - Selected isotopes and spectral
        interferences for quadrupole ICP-MS instruments
Bibliography

This Technical Specification specifies a method for the determination of the following elements in aqua regia or nitric acid digests of sludge, treated biowaste and soil:Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).The working range depends on the matrix and the interferences encountered. The limit of detection of the method is between 0,1 mg/kg dry matter and 2,0 mg/kg dry matter for most elements.The limit of detection will be higher in cases where the determination is likely to be interfered (see Clause 4) or in case of memory effects (see e.g. 8.2 of EN ISO 17294-1:2006).

Committee
CEN/TC 444
DevelopmentNote
Supersedes PREN 16171. (02/2013)
DocumentType
Technical Specification
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn
SupersededBy

CEN/TS 16637-3:2016 Construction products - Assessment of release of dangerous substances - Part 3: Horizontal up-flow percolation test
PD CEN/TS 16637-3:2016 Construction products. Assessment of release of dangerous substances Horizontal up-flow percolation test
S.R. CEN/TS 16637-3:2016 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 3: HORIZONTAL UP-FLOW PERCOLATION TEST

EN ISO 17294-1:2006 Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General guidelines (ISO 17294-1:2004)
EN 16174:2012 Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
ISO 17294-1:2004 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 1: General guidelines
EN 16173:2012 Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15934:2012 Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content

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