CEN/TS 16171:2012
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
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Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)
11-03-2023
21-11-2012
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Procedure
8 Calculation
9 Expression of results
10 Performance characteristics
11 Test report
Annex A (informative) - Selected isotopes and spectral
interferences for quadrupole ICP-MS instruments
Bibliography
This Technical Specification specifies a method for the determination of the following elements in aqua regia or nitric acid digests of sludge, treated biowaste and soil:Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).The working range depends on the matrix and the interferences encountered. The limit of detection of the method is between 0,1 mg/kg dry matter and 2,0 mg/kg dry matter for most elements.The limit of detection will be higher in cases where the determination is likely to be interfered (see Clause 4) or in case of memory effects (see e.g. 8.2 of EN ISO 17294-1:2006).
Committee |
CEN/TC 444
|
DevelopmentNote |
Supersedes PREN 16171. (02/2013)
|
DocumentType |
Technical Specification
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Withdrawn
|
SupersededBy |
Standards | Relationship |
XP CEN/TS 16171 : 2013 XP | Identical |
DIN SPEC 91256 : 2013 | Identical |
S.R. CEN/TS 16171:2012 | Identical |
DIN CEN/TS 16171;DIN SPEC 91256:2013-03 | Identical |
UNI CEN/TS 16171 : 2013 | Identical |
PNE-prEN 16171 | Identical |
CEN/TS 16637-3:2016 | Construction products - Assessment of release of dangerous substances - Part 3: Horizontal up-flow percolation test |
PD CEN/TS 16637-3:2016 | Construction products. Assessment of release of dangerous substances Horizontal up-flow percolation test |
S.R. CEN/TS 16637-3:2016 | CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 3: HORIZONTAL UP-FLOW PERCOLATION TEST |
EN ISO 17294-1:2006 | Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General guidelines (ISO 17294-1:2004) |
EN 16174:2012 | Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements |
ISO 17294-1:2004 | Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 1: General guidelines |
EN 16173:2012 | Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements |
ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
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