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BS 6068-2.99(2006) : 2006

Current

Current

The latest, up-to-date edition.

WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHERS IN SEDIMENT AND SEWAGE SLUDGE - METHOD USING EXTRACTION AND GAS CHROMATOGRAPHY/MASS SPECTROMETRY

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2006

$464.73
Including GST where applicable

Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
        in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
        electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography

Defines a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode.

Committee
EH/3/2
DevelopmentNote
Supersedes 04/30091620 DC. (02/2007) Also numbered as BS EN ISO 22032. (06/2009)
DocumentType
Standard
Pages
36
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
EN ISO 22032:2009 Identical
ISO 22032:2006 Identical

ISO 5667-13:2011 Water quality Sampling Part 13: Guidance on sampling of sludges
ISO/TR 13530:1997 Water quality Guide to analytical quality control for water analysis
EN 12880:2000 Characterization of sludges - Determination of dry residue and water content
DIN 32645:2008-11 CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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