ASTM E 1899 : 2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Hydroxyl Groups Using Reaction with p-Toluenesulfonyl Isocyanate (TSI) and Potentiometric Titration with Tetrabutylammonium Hydroxide
Hardcopy , PDF
17-06-2023
English
22-02-2019
Important note : All end users must be registered with an Account prior to user licenses being assigned.This test method covers the determination of hydroxyl groups attached to primary and secondary carbon atoms in aliphatic and cyclic compounds and phenols
| Committee |
D 16
|
| DocumentType |
Test Method
|
| Pages |
5
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method covers the determination of hydroxyl groups attached to primary and secondary carbon atoms in aliphatic and cyclic compounds and phenols. It is not suitable for determination of hydroxyl groups attached to tertiary carbon atoms. This test method is applicable to polyacetals, temperature sensitive materials, high solids polymer polyols, and rigid polyols. Other available test methods listed in Note 1 are not suitable for many of the sample types listed above.
1.1.1This test method is currently recommended for neutral refined products. Successful application has been made, however, to some in-process samples that contain an excess of acidic species. Proper validation must be performed, of course, to show that the acidic species either does not interfere, or that the acidic species interference has been obviated.
Note 1:Other methods for determination of hydroxyl groups are given in Test Methods D817, D871, D1957, D2195, D4252, D4273, D4274, E222, E326, and E335.
1.2Review the current appropriate Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.
1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated, with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazards see Section 9.
| ASTM D 6342 : 2022 | Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy |
| ASTM E 1547 : 2009 : R2023 | Standard Terminology Relating to Industrial and Specialty Chemicals |
| ASTM E 1547 : 2009 : R2017 | Standard Terminology Relating to Industrial and Specialty Chemicals |
| ASTM D 6342 : 2012 : R2017 : EDT 1 | Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy |
| ASTM D 4252 : 1989 : R2009 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 2195 : 2000 | Standard Test Methods for Pentaerythritol |
| ASTM D 4274 : 2005 | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
| ASTM D 4274 : 2011 | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
| ASTM E 222 : 2017 | Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation |
| ASTM D 4273 : 2023 | Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols |
| ASTM E 222 : 2023 | Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation |
| ASTM D 2195 : 2005 | Standard Test Methods for Pentaerythritol (Withdrawn 2011) |
| ASTM D 1957 : 1986 : R1995 : EDT 1 | Standard Test Method for Hydroxyl Value of Fatty Oils and Acids |
| ASTM D 1193 : 1977 : R1983 : EDT 1 | Standard Specification for Reagent Water |
| ASTM D 1193 : 2006 : R2011 | Standard Specification for Reagent Water |
| ASTM E 300 : 2003 : R2022 | Standard Practice for Sampling Industrial Chemicals |
| ASTM D 4273 : 2011 | Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols |
| ASTM D 4252 : 1989 : R2017 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 1193 : 1991 | Standard Specification for Reagent Water |
| ASTM D 1957 : 1986 : R2001 | Standard Test Method for Hydroxyl Value of Fatty Oils and Acids (Withdrawn 2007) |
| ASTM D 4252 : 1989 : R2003 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 4252 : 1989 : R1995 : EDT 1 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 4273 : 2018 | Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols |
| ASTM D 4273 : 1999 | Standard Test Methods for Polyurethane Raw Materials Determination of Primary Hydroxyl Content of Polyether Polyols |
| ASTM D 4273 : 2005 | Standard Test Methods for Polyurethane Raw Materials Determination of Primary Hydroxyl Content of Polyether Polyols |
| ASTM E 326 : 1996 | Test Method for Hydroxyl Groups by Phthalic Anhydride Esterification (Withdrawn 2001) |
| ASTM E 300 : 2003 : R2017 | Standard Practice for Sampling Industrial Chemicals |
| ASTM D 1193 : 1970 | Standard Specification For Reagent Water |
| ASTM D 4274 : 2016 | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
| ASTM D 1193 : 2006 | Standard Specification for Reagent Water |
| ASTM D 1193 : 1999 | Standard Specification for Reagent Water |
| ASTM D 1193 : 2006 : R2018 | Standard Specification for Reagent Water |
| ASTM D 4274 : 2021 | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
| ASTM D 4274 : 1999 | Standard Test Methods for Testing Polyurethane Raw Materials Determination of Hydroxyl Numbers of Polyols |
| ASTM E 335 : 1996 | Standard Test Method for Hydroxyl Groups by Pyromellitic Dianhydride Esterification (Withdrawn 2003) |
| ASTM D 4274 : 2023 | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
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