ASTM D 7596 : 2014
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Method for Automatic Particle Counting and Particle Shape Classification of Oils Using a Direct Imaging Integrated Tester
Available format(s)
Hardcopy , PDF
Superseded date
17-03-2023
Superseded by
Language(s)
English
Published date
16-12-2019
Important note : All end users must be registered with an Account prior to user licenses being assigned.1.1 This test method covers the determination of particle concentration, particle size distribution, particle shape, and soot content for new and in-service oils used for lubrication and hydraulic systems by a direct imaging integrated tester.
| Committee |
D 02
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| DocumentType |
Test Method
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| Pages |
7
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method covers the determination of particle concentration, particle size distribution, particle shape, and soot content for new and in-service oils used for lubrication and hydraulic systems by a direct imaging integrated tester.
1.1.1The test method is applicable to petroleum and synthetic based fluids. Samples from 2 to 150 mm2/s at 40°C may be processed directly. Samples of greater viscosity may be processed after solvent dilution.
1.1.2Particles measured are in the range from 4 μm to ≥ 70 μm with the upper limit dependent upon passing through a 100 μm mesh inlet screen.
1.1.3Particle concentration measured may be as high as 5 000 000 particles per mL without significant coincidence error.
1.1.4Particle shape is determined for particles greater than approximately 20 µm in length. Particles are categorized into the following categories: sliding, cutting, fatigue, nonmetallic, fibers, water droplets, and air bubbles.
1.1.5Soot is determined up to approximately 1.5 % by weight.
1.1.6This test method uses objects of known linear dimension for calibration.
1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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| ASTM E 3338 : 2022 | Standard Guide for Size and Shape of Solid Particles, Liquid Droplets, and Gas Bubbles, Dynamically Conveyed, Using a Dynamic Imaging Analyzer |
| ASTM D 7684 : 2011 : R2016 | Standard Guide for Microscopic Characterization of Particles from In-Service Lubricants |
| ASTM D 7720 : 2011 : R2017 | Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination |
| ASTM D 8128 : 2017 | Standard Guide for Monitoring Failure Mode Progression in Industrial Applications with Rolling Element Ball Type Bearings |
| ASTM D 4175 : 2020 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2014 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2015 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4057 : 2019 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 4175 : 2009 : REV A : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 2896 : 1998 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4175 : 2008 : REV B : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 2896 : 2005 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4057 : 1995 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6595 : 2016 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 4175 : 2005 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2019 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2005 : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2014 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 5967 : 2008 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4177 : 2016 : EDT 1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM G 40 : 2021 | Standard Terminology Relating to Wear and Erosion |
| ASTM D 5185 : 1997 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4175 : 2015 : REV C | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2009 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2020 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2017 : REV A : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 5967 : 2021 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4177 : 1995 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 4175 : 2008 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2020 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4057 : 2012 : R2018 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 5967 : 2012 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2017 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6304:2016 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration |
| ASTM D 4175 : 2009 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2003 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 6304 : 2004 : REV A : EDT 1 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM E 2412 : 2010 : R2018 | Standard Practice for Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry |
| ASTM D 4175 : 2022 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 5185 : 2005 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4175 : 2009 : REV A : EDT 4 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2009 : REV A : EDT 3 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4057 : 1981 : EDT 2 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 5967 : 2004 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 5185 : 2002 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 2896 : 2007 : REV A | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 445 : 2021 : EDT 2 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 4175 : 2018 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6304 : 2007 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration (Withdrawn 2016) |
| ASTM D 6304 : 2004 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM D 5185 : 2018 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 7279 : 2016 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 2896 : 2011 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4175 : 2001 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2020 : REV B : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6595 : 2000 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 4175 : 2001 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2005 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 6304 : 2016 : EDT 1 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration |
| ASTM D 4175 : 2022 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2002 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5185 : 2013 : EDT 1 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 6304 : 2004 : REV A | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM D 445 : 1988 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity) |
| ASTM D 6304 : 2004 : EDT 1 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM D 5967 : 2015 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 7279 : 2018 : EDT 1 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 4057 : 2006 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 7279 : 2018 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 4175 : 2015 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2002 : REV A : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4177 : 2015 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6304 : 2000 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM D 4057 : 2012 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 2896 : 2001 : EDT 1 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 5185 : 2013 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4175 : 2009 : REV A : EDT 5 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV C | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6595 : 2000 : R2011 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 5967 : 2011 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2015 : REV B | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 7279 : 2014 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 2896 : 2001 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4175 : 2015 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5967 : 2017 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM G 40 : 2021 : REV A | Standard Terminology Relating to Wear and Erosion |
| ASTM D 445 : 2019 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 4177 : 2022 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 7279 : 2006 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 4175 : 2009 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 2896 : 2003 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4177 : 1995 : R2010 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 4175 : 2002 : REV A : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2008 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 6595 : 2022 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 4175 : 2002 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4177 : 1995 : R2000 | Standard Practice for Automatic Sampling of Peroleum and Petroleum Products |
| ASTM D 4175 : 2000 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 5967 : 2007 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 2896 : 2006 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 5967 : 2010 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 6595 : 2000 : R2005 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 4175 : 2019 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6304 : 2003 | Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fisher Titration |
| ASTM D 4175 : 2022 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM G 40 : 2022 | Standard Terminology Relating to Wear and Erosion |
| ASTM E 2412 : 2010 | Standard Practice for Condition Monitoring of Used Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry |
| ASTM D 5185 : 2009 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 445 : 2001 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity) |
| ASTM D 445 : 2021 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM G 40 : 2022 : REV A | Standard Terminology Relating to Wear and Erosion |
| ASTM D 2896 : 2015 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM E 2412 : 2004 | Standard Practice for Condition Monitoring of Used Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry |
| ASTM D 5967 : 2013 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 5967 : 2012 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2017 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6595 : 2017 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 4057 : 2022 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 5967 : 2005 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 2896 : 2007 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4175 : 2009 : REV A : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4177 : 2016 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 5185 : 2002 : EDT 1 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 7279 : 2020 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 4177 : 2020 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 4177 : 1995 : R2005 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 4175 : 2018 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2016 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 5967 : 2010 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 5185 : 2002 : EDT 2 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 7279 : 2014 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 445 : 2021 : EDT 1 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM G 40 : 2017 | Standard Terminology Relating to Wear and Erosion |
| ASTM D 4057 : 1995 : R2000 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 5967 : 1999 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
| ASTM D 4175 : 2017 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7279 : 2008 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 4175 : 2019 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4177 : 2015 : REV A | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 2896 : 2021 | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ASTM D 4057 : 2006 : R2011 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 4175 : 2015 : REV B : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2008 : REV B | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
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