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ASTM D 6299 : 2013

NA

NA

Status of Standard is Unknown

Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-10-2013

$176.78
Including GST where applicable

Committee
D 02
DocumentType
Standard Practice
Pages
28
PublisherName
American Society for Testing and Materials
Status
NA
SupersededBy
Supersedes

1.1This practice covers information for the design and operation of a program to monitor and control ongoing stability and precision and bias performance of selected analytical measurement systems using a collection of generally accepted statistical quality control (SQC) procedures and tools.

Note 1A complete list of criteria for selecting measurement systems to which this practice should be applied and for determining the frequency at which it should be applied is beyond the scope of this practice. However, some factors to be considered include (1) frequency of use of the analytical measurement system, (2) criticality of the parameter being measured, (3) system stability and precision performance based on historical data, (4) business economics, and (5) regulatory, contractual, or test method requirements.

1.2This practice is applicable to stable analytical measurement systems that produce results on a continuous numerical scale.

1.3This practice is applicable to laboratory test methods.

1.4This practice is applicable to validated process stream analyzers.

1.5This practice is applicable to monitoring the differences between two analytical measurement systems that purport to measure the same property provided that both systems have been assessed in accordance with the statistical methodology in Practice D6708 and the appropriate bias applied.

Note 2For validation of univariate process stream analyzers, see also Practice D3764.
Note 3One or both of the analytical systems in 1.5 can be laboratory test methods or validated process stream analyzers.

1.6This practice assumes that the normal (Gaussian) model is adequate for the description and prediction of measurement system behavior when it is in a state of statistical control.

Note 4For non-Gaussian processes, transformations of test results may permit proper application of these tools. Consult a statistician for further guidance and information.

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ASTM D 4951 : 2014 Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 4927 : 2015 Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy
ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
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ASTM D 6278 : 2017 : EDT 1 Standard Test Method for Shear Stability of Polymer Containing Fluids Using a European Diesel Injector Apparatus
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 1218 : 2012 : R2016 Standard Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids
ASTM D 8001 : 2016 : EDT 1 Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography
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ASTM D 6378 : 2018 : REV A Standard Test Method for Determination of Vapor Pressure (VP<inf>X</inf>) of Petroleum Products, Hydrocarbons, and Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method)
ASTM D 6443 : 2014 : R2019 : EDT 1 Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
ASTM D 3831 : 2012 : R2017 Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
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ASTM D 7314 : 2010 : R2015 Standard Practice for Determination of the Heating Value of Gaseous Fuels using Calorimetry and On-line/At-line Sampling
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ASTM D 7042 : 2016 : EDT 3 Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)
ASTM D 4045 : 2015 Standard Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry
ASTM D 8174 : 2018 Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small-Scale Closed Cup Tester
ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 4629 : 2017 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 4628 : 2016 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
ASTM D 1552 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 7808 : 2018 Standard Practice for Determining the Site Precision of a Process Stream Analyzer on Process Stream Material
ASTM D 7279 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer
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ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 909 : 2018 Standard Test Method for Supercharge Rating of Spark-Ignition Aviation Gasoline
ASTM D 94 : 2007 : R2017 Standard Test Methods for Saponification Number of Petroleum Products
ASTM D 8146 : 2018 Standard Guide for Evaluating Test Method Capability and Fitness for Use
ASTM D 2885 : 2019 : REV A Standard Test Method for Determination of Octane Number of Spark-Ignition Engine Fuels by On-Line Direct Comparison Technique
ASTM D 7845 : 2017 Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography/Mass Spectrometry
ASTM D 5188 : 2016 Standard Test Method for Vapor-Liquid Ratio Temperature Determination of Fuels (Evacuated Chamber and Piston Based Method)
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ASTM F 2853 : 2010 : R2015 Standard Test Method for Determination of Lead in Paint Layers and Similar Coatings or in Substrates and Homogenous Materials by Energy Dispersive X-Ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams
ASTM D 6792 : 2017 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 7166 : 2010 : R2015 Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
ASTM D 7164 : 2010 : R2015 Standard Practice for On-line/At-line Heating Value Determination of Gaseous Fuels by Gas Chromatography
ASTM D 6897 : 2016 Standard Test Method for Vapor Pressure of Liquefied Petroleum Gases (LPG) (Expansion Method)
ASTM D 7345 : 2017 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Micro Distillation Method)
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ASTM D 2699 : 2019 Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
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ASTM D 3828 : 2016 : REV A Standard Test Methods for Flash Point by Small Scale Closed Cup Tester
ASTM F 2980 : 2013 : R2017 Standard Test Method for Analysis of Heavy Metals in Glass by Field Portable X-Ray Fluorescence (XRF)
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ASTM D 613 : 2018 : REV A Standard Test Method for Cetane Number of Diesel Fuel Oil
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ASTM D 6708 : 2019 Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
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ASTM D 1318 : 2016 Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method)
ASTM D 1266 : 2018 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
ASTM D 7875 : 2014 Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
ASTM D 6890 : 2018 Standard Test Method for Determination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustion in a Constant Volume Chamber
ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6895 : 2017 Standard Test Method for Rotational Viscosity of Heavy Duty Diesel Drain Oils at 100 °C
ASTM F 2617 : 2015 Standard Test Method for Identification and Quantification of Chromium, Bromine, Cadmium, Mercury, and Lead in Polymeric Material Using Energy Dispersive X-ray Spectrometry
ASTM D 6728 : 2016 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 4323 : 2015 Standard Test Method for Hydrogen Sulfide in the Atmosphere by Rate of Change of Reflectance
ASTM D 6732 : 2004 : R2015 Standard Test Method for Determination of Copper in Jet Fuels by Graphite Furnace Atomic Absorption Spectrometry
ASTM D 7756 : 2019 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection
ASTM D 6849 : 2013 Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 1091 : 2011 : R2016 Standard Test Methods for Phosphorus in Lubricating Oils and Additives (Withdrawn 2021)
ASTM D 7235 : 2016 Standard Guide for Establishing a Linear Correlation Relationship Between Analyzer and Primary Test Method Results Using Relevant ASTM Standard Practices
ASTM D 7220 : 2012 : R2017 Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 7260 : 2019 Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 3341 : 2016 Standard Test Method for Lead in Gasoline—Iodine Monochloride Method (Withdrawn 2022)
ASTM D 7923 : 2019 Standard Test Method for Water in Ethanol and Hydrocarbon Blends by Karl Fischer Titration
ASTM D 5184 : 2012 : R2017 Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
ASTM E 1655 : 2017 Standard Practices for Infrared Multivariate Quantitative Analysis
ASTM D 7111 : 2016 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 3244 : 2018 Standard Practice for Utilization of Test Data to Determine Conformance with Specifications
ASTM D 7170 : 2016 Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Fixed Range Injection Period, Constant Volume Combustion Chamber Method (Withdrawn 2019)
ASTM D 4294 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 3120 : 2008 : R2019 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
ASTM D 7040 : 2004 : R2015 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 8267 : 2019 Standard Test Method for Determination of Saturated Hydrocarbon, Aromatic, and Diaromatic Content of Aviation Turbine Fuels Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
ASTM D 8185 : 2018 Standard Guide for In-Service Lubricant Viscosity Measurement
ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
ASTM D 7622 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 5863 : 2000 : REV A : R2016 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 8088 : 2016 Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy
ASTM D 1018 : 2011 : R2016 Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021)
ASTM D 7828 : 2012 Standard Test Method for Determination of Residue Composition in Liquefied Petroleum Gas (LPG) Using Automated Thermal Desorption/Gas Chromatography (ATD/GC) (Withdrawn 2021)
ASTM D 5708 : 2015 Standard Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry
ASTM D 7807 : 2012 Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
ASTM D 5501 : 2012 : R2016 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
ASTM D 6550 : 2015 Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography
ASTM D 8071 : 2017 Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
ASTM D 6375 : 2009 : R2014 Standard Test Method for Evaporation Loss of Lubricating Oils by Thermogravimetric Analyzer (TGA) Noack Method
ASTM D 6450 : 2016 : REV A Standard Test Method for Flash Point by Continuously Closed Cup (CCCFP) Tester
ASTM D 5600 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 7303 : 2017 Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7236 : 2016 : REV A Standard Test Method for Flash Point by Small Scale Closed Cup Tester (Ramp Method)
ASTM D 3606 : 2017 Standard Test Method for Determination of Benzene and Toluene in Spark Ignition Fuels by Gas Chromatography
ASTM D 7551 : 2010 : R2015 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases and Natural Gas by Ultraviolet Fluorescence (Withdrawn 2024)
ASTM E 2313 : 2015 Standard Test Method for Aldehydes in Mono-, Di-, and Triethylene Glycol (using Spectrophotometry)
ASTM D 5056 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM D 7039 : 2015 : REV A Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 5186 : 2019 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
ASTM D 6617 : 2017 Standard Practice for Laboratory Bias Detection Using Single Test Result from Standard Material
ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM D 7806 : 2012 Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy

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