ASTM D 3257 : 2006 : R2012
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
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Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography (Withdrawn 2021)
Hardcopy , PDF
25-01-2021
English
07-08-2012
CONTAINED IN VOL. 06.04, 2017 Determines the ethylbenzene and total eight-carbon (C[8]) and heavier aromatics in the concentration range from 0.1 to 30% in mineral spirits having a distillation range from 149 to 210 degrees C (300 to 410 degrees F) as determined by Test Method D 86.
Committee |
D 01
|
DocumentType |
Test Method
|
Pages |
8
|
ProductNote |
Reconfirmed 2012
|
PublisherName |
American Society for Testing and Materials
|
Status |
Withdrawn
|
SupersededBy | |
Supersedes |
1.1These test methods cover the determination of ethylbenzene and total eight-carbon (C8) and heavier aromatics in the concentration range from 0.1 to 30 % in mineral spirits having a distillation range from 149 to 210°C (300 to 410°F) as determined by Test Method D86. The procedures permit the identification and calculation of concentrations of aromatic components to 0.1 volume %.
1.2It is recognized by analytical chemists that a single column gas chromatography analysis of an unknown sample is risky. In such cases, multiple and different analytical techniques must be used for absolutely positive identification, for example, several different gas chromatography columns, gas chromatography/mass spectrometer, or gas chromatography/infrared, etc. In these test methods the material is known and is clearly defined.
1.3Oxygenated compounds, if present, may interfere and cause erroneous results. Such oxygenated compounds are not normally present in mineral spirits.
1.4Three test methods are covered as follows:
1.4.1Test Method A, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene), and total aromatics by means of a single packed column gas chromatographic analysis.
1.5The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.6For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
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ASTM D 268 : 2001 : R2012 | Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material (Withdrawn 2021) |
ASTM D 235 : 2002 : R2012 | Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent) (Withdrawn 2021) |
ASTM D 235 : 2022 | Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent) |
ASTM D 268 : 2022 | Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material |
ASTM E 260 : 1996 | Standard Practice for Packed Column Gas Chromatography |
ASTM D 86 : 2017-06 | TEST METHOD FOR DISTILLATION OF PETROLEUM PRODUCTS AND LIQUID FUELS AT ATMOSPHERIC PRESSURE |
ASTM E 180 : 2003 | Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009) |
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