ASTM D 2036 : 2009 : R2022
Current
The latest, up-to-date edition.
Standard Test Methods for Cyanides in Water
Hardcopy , PDF
English
13-05-2022
Committee |
D 19
|
DocumentType |
Test Method
|
Pages |
20
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1These test methods cover the determination of cyanides in water. The following test methods are included:
Sections | |
Test Method A | 12 – 18 |
Test Method B | 19 – 25 |
Test Method C | 26 – 32 |
Test Method D | 33 – 39 |
1.2Cyanogen halides may be determined separately.
Note 1:Cyanogen chloride is the most common of the cyanogen halide complexes as it is a reaction product and is usually present when chlorinating cyanide-containing industrial waste water. For the presence or absence of CNCl, the spot test method given in Annex A1 can be used.
1.3These test methods do not distinguish between cyanide ions and metallocyanide compounds and complexes. Furthermore, they do not detect the cyanates. Cyanates can be determined using ion chromatography without digestion.
Note 2:The cyanate complexes are decomposed when the sample is acidified in the distillation procedure.
1.4The cyanide in cyanocomplexes of gold, platinum, cobalt and some other transition metals is not completely recovered by these test methods. Refer to Test Method D6994 for the determination of cyanometal complexes.
1.5Cyanide from only a few organic cyanides are recovered, and those only to a minor extent.
1.6Part or all of these test methods have been used successfully with reagent water and various waste waters. It is the user's responsibility to assure the validity of the test method for the water matrix being tested.
1.7The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 5.1, 8.8, 8.18, Section 9, 11.3, and 16.1.9.
1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D 7572 : 2015 : R2022 | Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil |
ASTM D 4165 : 2006 : R2020 : EDT 1 | Standard Test Method for Cyanogen Chloride in Water |
ASTM D 4193 : 2008 : R2020 : EDT 1 | Standard Test Method for Thiocyanate in Water |
ASTM D 7511 : 2012 : R2017 : EDT 1 | Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection |
ASTM D 7284 : 2020 | Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection |
ASTM D 7237 : 2018 | Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection |
ASTM E 800 : 2020 | Standard Guide for Measurement of Gases Present or Generated During Fires |
ASTM D 7295 : 2018 | Standard Practice for Sampling Combustion Effluents and Other Stationary Sources for the Subsequent Determination of Hydrogen Cyanide |
ASTM D 7728 : 2018 | Standard Guide for Selection of ASTM Analytical Methods for Implementation of International Cyanide Management Code Guidance |
ASTM D 3694 : 1996 : R2017 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
ASTM D 6888 : 2016 | Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection |
ASTM D 5788 : 1995 : R2017 | Standard Guide for Spiking Organics into Aqueous Samples |
ASTM D 1129 : 2013 : R2020 | Standard Terminology Relating to Water |
ASTM D 1129 : 2013 : R2020 : EDT 2 | Standard Terminology Relating to Water |
ASTM D 6696 : 2016 | Standard Guide for Understanding Cyanide Species |
ASTM D 2777 : 2021 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
ASTM D 2777 : 2013 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
ASTM D 1129 : 2013 : R2020 : EDT 1 | Standard Terminology Relating to Water |
ASTM E 60 : 2011 : R2016 | Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry |
ASTM D 5847 : 2002 : R2020 | Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis |
ASTM D 5788 : 1995 : R2024 | Standard Guide for Spiking Organics into Aqueous Samples |
ASTM D 6888 : 2016 : R2023 | Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection |
ASTM D 6696 : 2016 : R2023 | Standard Guide for Understanding Cyanide Species |
ASTM D 5847 : 2022 | Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis |
ASTM D 7365 : 2009 : REV A : R2015 | Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide |
ASTM E 60 : 2011 : R2022 : EDT 1 | Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry |
ASTM D 6994 : 2015 | Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection (Withdrawn 2024) |
ASTM D 7365 : 2009 : REV A : R2022 | Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide |
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