ASTM C 1108 : 2017
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Plutonium by Controlled-Potential Coulometry
Hardcopy , PDF
23-08-2022
English
17-11-2017
Important note : All end users must be registered with an Account prior to user licenses being assigned.| Committee |
C 26
|
| DocumentType |
Test Method
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| Pages |
9
|
| PublisherName |
American Society for Testing and Materials
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| Status |
Superseded
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| SupersededBy | |
| Supersedes |
1.1This test method describes the determination of dissolved plutonium from unirradiated nuclear-grade (that is, high-purity) materials by controlled-potential coulometry. Controlled-potential coulometry may be performed in a choice of supporting electrolytes, such as 0.9 M HNO3, 1 M HClO4, 1 M HCl, 5 M HCl, and 0.5 M H2SO4. Limitations on the use of selected supporting electrolytes are discussed in Section 6. Optimum quantities of plutonium for this procedure are 5 to 20 mg.
1.2Plutonium-bearing materials are radioactive and toxic. Adequate laboratory facilities, such as gloved boxes, fume hoods, controlled ventilation, etc., along with safe techniques must be used in handling specimens containing these materials.
1.3The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM C 758 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal |
| ASTM C 759 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions |
| ASTM C 1165 : 2017 | Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode |
| ASTM C 697 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets |
| ASTM C 698 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O<inf>2</inf>) |
| ASTM C 1128 : 2018 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1009 : 2013 : REV A | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
| ASTM C 1210 : 2018 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM C 859 : 2014 : REV B | Standard Terminology Relating to Nuclear Materials |
| ASTM C 1009 : 1996 : EDT 1 | Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005) |
| ASTM C 1210 : 1996 : EDT 1 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005) |
| ASTM C 1210 : 2021 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry |
| ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM C 1128 : 1995 : EDT 1 | Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1068 : 1996 : EDT 1 | Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry |
| ASTM C 1168 : 2015 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM C 1128 : 2015 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM C 1068 : 2015 | Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry |
| ASTM C 1068 : 2021 | Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry |
| ASTM E 691 : 2022 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM C 859 : 2022 | Standard Terminology Relating to Nuclear Materials |
| ASTM C 859 : 2022 : REV A | Standard Terminology Relating to Nuclear Materials |
| ASTM C 1297 : 1995 : EDT 1 | Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials |
| ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM C 1156 : 1995 : EDT 1 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM C 1168 : 1990 : R1995 : EDT 1 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM C 1009 : 2021 | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
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