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AS 4969.1-2008

Current

Current

The latest, up-to-date edition.

Analysis of acid sulfate soil - Dried samples - Methods of test Pre-treatment of samples

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

English

Published date

30-06-2008

$59.99
Including GST where applicable

This Standard provides a procedure for pre-treating acid sulfate soil following sampling, prior to their analysis as dried sample using appropriate methods of test. The procedure includes the handling of samples before delivery to the laboratory, and the drying, grinding and storage of samples. The Standard also provides a procedure for archiving a sample after analysis.

Committee
EV-009
DocumentType
Standard
ISBN
0 7337 8720 7
Pages
6
ProductNote
Reconfirmed 25/05/2018.This standard has been reconfirmed in Australia in 2018 and remains current in New Zealand. Reconfirmation Notice 25/05/2018
PublisherName
Standards Australia
Status
Current
Supersedes

This Standard provides a procedure for pre-treating acid sulfate soil following sampling, prior to their analysis as dried sample using appropriate methods of test. The procedure includes the handling of samples before delivery to the laboratory, and the drying, grinding and storage of samples. The Standard also provides a procedure for archiving a sample after analysis.NOTES:1 It is recommended to collect a field sample that provides approximately 200 g of dried sample.2 Field personnel may remove coarse fragments (e.g. shell, stones, rock fragments (2 mm) prior to sending the field sample to the laboratory. The presence of such fragments, their size, shape and abundance (and whether they have been removed) should be recorded in field sampling notes.3 For the chemical analysis to most closely reflect the condition of the acid sulfate soil in its natural state at the time of sampling, the handling, preparation and storage of these soils should be such that potential for oxidation of pyrite is minimized. 4 This method is not appropriate for preservation of acid volatile sulfur (e.g. iron monosulfides) in acid sulfate soil as oxidation of these compounds is likely to occur. This method, however, is suitable for the purpose of acid base accounting.

First published as AS 4969.1-2008.

AS/NZS 2243.1:2005 Safety in laboratories Planning and operational aspects
AS/NZS 2243.2:2006 Safety in laboratories Chemical aspects
AS 4969.0-2008 Analysis of acid sulfate soil - Dried samples - Methods of test Introduction and definitions, symbols and acronyms
AS/NZS 2243.3:2002 Safety in laboratories Microbiological aspects and containment facilities

AS 4969.3-2008 Analysis of acid sulfate soil - Dried samples - Methods of test Determination of peroxide pH (pHox), titratable peroxide acidity (TPA) and excess acid neutralizing capacity (ANCE)
AS 4969.2-2008 Analysis of acid sulfate soil - Dried samples - Methods of test Determination of pH
AS 4969.12-2009 Analysis of acid sulfate soil - Dried samples - Methods of test Complete suspension peroxide oxidation combined acidity and sulfur (SPOCAS) method (Reconfirmed 2018)
AS 4969.13-2009 Analysis of acid sulfate soil - Dried samples - Methods of test Determination of acid neutralizing capacity by back-titration (ANCBT) (Reconfirmed 2022)
AS 4969.7-2008 Analysis of acid sulfate soil - Dried samples - Methods of test Determination of chromium reducible sulfur (SCR) (Reconfirmed 2018)
AS 4969.8-2008 Analysis of acid sulfate soil - Dried samples - Methods of test Determination of hydrochloric acid extractable sulfur (SHCl), calcium (CaHCl) and magnesium (MgHCl) (Reconfirmed 2018)

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