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AS 1038.11-2002

AS 1038.11-2002

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Coal and coke - Analysis and testing Coal - Forms of sulfur (Reconfirmed 2013)

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Withdrawn date

10-11-2023

Language(s)

English

Published date

13-11-2002

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 1038.11-2002 COAL AND COKE-ANALYSIS AND TESTING - COAL-FORMS OF SULFUR
4 - PREFACE
5 - CONTENTS
6 - FOREWORD
7 - SECTION 1 SCOPE AND GENERAL
7 - 1.1 SCOPE
7 - 1.2 REFERENCED DOCUMENTS
7 - 1.3 DEFINITIONS
8 - 1.4 PRINCIPLE
8 - 1.5 SAFETY
8 - 1.6 SAMPLE
8 - 1.6.1 General
9 - 1.6.2 Equilibration
9 - 1.7 REPORTING OF RESULTS
9 - 1.8 PRECISION
9 - 1.9 TEST REPORT
10 - SECTION 2 DETERMINATION OF SULFATE SULFUR
10 - 2.1 PRINCIPLE
10 - 2.2 REAGENTS
10 - 2.2.1 General
10 - 2.2.2 Hydrochloric acid (rho20 1.18 g/mL)
10 - 2.2.3 Hydrochloric acid (rho20 1.18 g/mL) diluted 1 + 1
10 - 2.2.4 Ammonia solution (rho20 0.88 g/mL) diluted 1 + 2
10 - 2.2.5 Barium chloride solution (100 g/L)
10 - 2.2.6 Potassium sulfate solution (2 g/L)
10 - 2.2.7 Methyl red indicator solution (0.2 g/L)
10 - 2.2.8 Wetting agent
10 - 2.3 APPARATUS
10 - 2.3.1 General
10 - 2.3.2 Weighing device
10 - 2.3.3 Extraction flask
10 - 2.3.4 Condenser
11 - 2.3.5 Muffle furnace
11 - 2.3.6 Plate
11 - 2.3.7 Silica crucible
11 - 2.4 PROCEDURE
11 - 2.4.1 Number of determinations
11 - 2.4.2 Blank test
11 - 2.4.3 Determination
12 - 2.5 CALCULATION
13 - SECTION 3 DETERMINATION OF PYRITIC SULFUR
13 - 3.1 PRINCIPLE
13 - 3.2 EXTRACTION OF THE PYRITIC IRON
13 - 3.2.1 Reagents
13 - 3.2.2 Apparatus
13 - 3.2.3 Procedure
14 - 3.3 DETERMINATION OF PYRITIC IRON-TITRIMETRIC METHOD
14 - 3.3.1 Reagents
15 - 3.3.2 Apparatus
15 - 3.3.3 Determination
16 - 3.3.4 Calculation of result
16 - 3.4 DETERMINATION OF PYRITIC IRON-SPECTROPHOTOMETRIC METHOD
16 - 3.4.1 Reagents
16 - 3.4.2 Apparatus
17 - 3.4.3 Procedure
17 - 3.4.4 Preparation of calibration graph
18 - 3.4.5 Calculation of result
18 - 3.5 DETERMINATION OF PYRITIC IRON-ATOMIC ABSORPTION SPECTROMETRIC METHOD
18 - 3.5.1 Reagents
18 - 3.5.2 Apparatus
18 - 3.5.3 Procedure
19 - 3.5.4 Calibration graph
19 - 3.5.5 Calculation of result
20 - SECTION 4 ORGANIC SULFUR
21 - APPENDIX A - DERIVATION OF FACTORS USED IN THE CALCULATIONS
21 - A1 GENERAL
21 - A2 SULFATE SULFUR (see Clause 2.5)
21 - A3 PYRITIC SULFUR-TITRIMETRIC (see Clause 3.3.4)
22 - A4 PYRITIC SULFUR-SPECTROPHOTOMETRIC (see Clause 3.4.5)
22 - A5 PYRITIC SULFUR-ATOMIC ABSORPTION (see Clause 3.5.5)

Sets out methods for the determination of sulfate sulfur, pyritic sulfur and organic sulfur in coal.

Committee
MN-001
DocumentType
Standard
ISBN
0 7337 4916 X
Pages
16
ProductNote
Reconfirmed 06-08-2013
PublisherName
Standards Australia
Status
Withdrawn
Supersedes

This Standard sets out methods for the determination of sulfate sulfur, pyritic sulfur and organic sulfur in coal. The methods are as follows: (a) Sulfate sulfur is determined directly as a sulfate in a hydrochloric acid extract of the sample. (b) Pyritic sulfur is calculated from the determination of iron soluble in nitric acid following removal of non-pyritic iron by hydrochloric acid. (c) Organic sulfur is obtained by subtracting the sum of the pyritic sulfur and sulfate sulfur from the total sulfur, determined by one of the methods given in AS 1038.6.3.

Standards Relationship
ISO 157:1996 Identical

Originated as AS K152.11-1965.
Previous edition AS 1038.11-1993.
Fourth edition 2002.

AS 2508.6.020-1991 Safe storage and handling information card - Selenious acid, selenates and selenites
AS 2243.9-1991 Safety in laboratories - Recirculating fume cabinets
AS 2508.3.017-1983 Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.3.027-1983 Safe storage and handling information card - Diacetone alcohol
AS 2508.6.002-1985 Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.3.008-1983 Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.2.007-2001 Safe storage and handling information card - Liquefied petroleum gas
AS 2508.3.010-1995 Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 3753-2001 Recommended practice for chemical analysis by ultraviolet/visible spectrophotometry
AS 2508.3.012-1982 Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.3.015-1992 Safe storage and handling information card - Toluene (toluol)
AS 2508.6.017-1989 Safe storage and handling information card - Lead acetate
AS 2243.3-1991 Safety in laboratories Microbiology
AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures
AS 2508.3.014-1992 Safe storage and handling information card - Xylenes (xylols)
AS 2508.3.011-1992 Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.2.013-1992 Safe storage and handling information card - Ethylene (ethene)
AS 2508.3.033-1984 Safe storage and handling information card - Isoprene, inhibited
AS 2508.3.016-1982 Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
AS 2243.10-1993 Safety in laboratories - Storage of chemicals
AS 2508.6.011-1988 Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2508.6.019-1995 Safe storage and handling information card - Lead alkyls
AS 2508.3.018-1983 Safe storage and handling information card - Methyl isobutyl carbinol
AS 2508.3.019-1983 Safe storage and handling information card - Methacrylates, HFP
AS 2243.6-1990 Safety in laboratories - Mechanical aspects
AS 2508.2.008-1984 Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992 Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.5.004-1991 Safe storage and handling information card - Benzoyl peroxide
AS 2508.8.014-1985 Safe storage and handling information card - Mercury metal
AS 2508.5.005-1992 Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2508.10.001-2000 Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2243.4-1998 Safety in laboratories - Ionizing radiations
AS 2508.6.022-1986 Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.6.001-1988 Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 2508.3.026-1995 Safe storage and handling information card - Propylene oxide
AS 2243.1-1990 Safety in laboratories General
AS 1038.6.3.2-2003 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)
AS 2508.2.010-1984 Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.6.008-1989 Safe storage and handling information card - Ammonium thioglycolate
AS 2508.3.009-1982 Safe storage and handling information card - Hydrocarbon solvents
AS 2508.3.034-1984 Safe storage and handling information card - Pentanes
AS 2508.6.009-1990 Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 2508.8.015-1988 Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.8.017-1988 Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2706-2003 Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
AS 2508.3.029-1983 Safe storage and handling information card - Glycol ethers (flammable)
AS 2508.8.010-1990 Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 1038.6.3.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method
AS 2508.8.005-1992 Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.3.028-1983 Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995 Safe storage and handling information card - Acetic anhydride
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 2508.6.012-1988 Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.6.005-1984 Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.2.006-1995 Safe storage and handling information card - Ethylene oxide
AS 2508.8.018-1995 Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.013-1991 Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.5.001-1989 Safe storage and handling information card - Hydrogen peroxide
AS 2508.6.006-1982 Safe storage and handling information card - Beryllium and compounds
AS 2508.6.027-1984 Safe storage and handling information card - Tributyltin-oxide
AS 2508.8.003-1990 Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.3.004-1982 Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 1038.6.3.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - Eschka method (Reconfirmed 2013)
AS 2508.2.005-1984 Safe storage and handling information card - Chlorine (compressed)
AS 2508.8.008-1992 Safe storage and handling information card - Maleic anhydride
AS 2243.8-1992 Safety in laboratories Fume cupboards
AS 2508.6.013-1991 Safe storage and handling information card - Trichloroethylene
AS 2508.3.013-1984 Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.3.024-1995 Safe storage and handling information card - Dimethylamine solution
AS 2508.8.002-1986 Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2508.8.004-1992 Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.2.011-1984 Safe storage and handling information card - Butadiene (inhibited)
AS 2508.6.018-1989 Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
AS 2508.6.021-1984 Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.2.001-1992 Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.2.009-1984 Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2508.3.025-1983 Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 2508.3.032-1984 Safe storage and handling information card - Glycol ether acetates
AS 2508.6.023-1989 Safe storage and handling information card - Phenylmercuric compounds
AS 2508.8.016-1988 Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.2.004-1995 Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.2.002-1992 Safe storage and handling information card - Hydrogen (compressed)
AS 2508.6.014-1989 Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.3.001-1982 Safe storage and handling information card - Acetone
AS 2508.6.026-1984 Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS 2508.3.007-1995 Safe storage and handling information card - Carbon disulphide
AS 2508.3.006-1995 Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.8.009-1990 Safe storage and handling information card - Sulfuric acid (Oleum)
AS 2508.6.025-1984 Safe storage and handling information card - Arsenic acid
AS 2508.6.007-1995 Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS 2508.2.003-1995 Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.8.011-1995 Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.3.005-1995 Safe storage and handling information card - Benzene
AS 2508.3.020-1983 Safe storage and handling information card - Ethyl benzene
AS 2508.3.023-1983 Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2508.3.022-1983 Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.3.021-1983 Safe storage and handling information card - Cyclohexanone
AS 2508.6.010-1983 Safe storage and handling information card - Toluene diisocyanate (TDI)
AS 2508.5.002-1990 Safe storage and handling information card - Ammonium nitrate
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2508.6.028-1988 Safe storage and handling information card - Chloropicrin
AS 2508.8.012-1991 Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2243.7-1991 Safety in laboratories - Electrical aspects
AS 2508.6.016-1995 Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.4.001-1982 Safe storage and handling information card - Calcium carbide
AS 2508.3.003-1982 Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 2508.3.030-1983 Safe storage and handling information card - Cyclohexane
AS 2508.6.024-1984 Safe storage and handling information card - Pentachlorophenol
AS 2508.6.003-1984 Safe storage and handling information card - Aniline (aminobenzene)
AS 2508.6.004-1984 Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.8.007-1990 Safe storage and handling information card - Nitric acid
AS 2508.5.003-1990 Safe storage and handling information card - Calcium hypochlorite
AS 2508.6.015-1983 Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 1038.6.3.3-1997 Coal and coke - Analysis and testing Higher rank coal - Ultimate analysis - Total sulfur - Infrared method (Reconfirmed 2013)
AS 2508.2.012-1985 Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2134.1-1999 Recommended practice for chemical analysis by atomic absorption spectrometry Flame atomic absorption spectrometry (Reconfirmed 2016)
AS 2508.3.031-1983 Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.3.002-1982 Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990 Safety in laboratories - Chemical aspects
AS 2243.5-1993 Safety in laboratories Non-ionizing radiations

AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 4156.3-1994 Coal preparation Magnetite for coal preparation plant use - Test methods
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
AS 4156.3-2008 Coal preparation Magnetite for coal preparation plant use - Test methods (Reconfirmed 2020)
AS 1038.22-2000 Coal and coke - Analysis and testing Higher rank coal - Mineral matter and water of constitution (Reconfirmed 2013) (Reconfirmed 2023)
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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